Silver-Promoted Site-Selective Intramolecular Cyclization of 2-Methylthiobenzamide Through α-C(sp3)–H Functionalization
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2019-11
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English
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ACS
Abstract
Silver-mediated intramolecular α-C(sp3)–H bond functionalization of the methylthio group has been established in the presence of Selectfluor as an additive. This novel strategy provides efficient access to various diverse sulfur-based heterocycles with good yields and functional group compatibility. It is noteworthy that the completely novel benzooxathiin-4-imine skeletons were reported for the first time in this study.
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Yang, K., Niu, B., Ma, Z., Wang, H., Lawrence, B., & Ge, H. (2019). Silver-promoted site-selective intramolecular cyclization of 2-methylthiobenzamide through α-C(sp3)–H functionalization. The Journal of Organic Chemistry. https://doi.org/10.1021/acs.joc.9b02202
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The Journal of Organic Chemistry
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