Browsing by Author "Lee, J H"

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    Lamellar to Rod Eutectic Transition in the Hypereutectic Nickel- Aluminum Alloy
    (2014) Que, Z P; Gu, J H; Shin, J H; Choi, H K; Jung, Y G; Lee, J H
    Directional solidification experiments were carried out on the hypereutectic Ni-25 at.% Al alloy to examine the effect of growth velocity on the eutectic microstructure. The growth velocity was varied from 1 to 20 μm/s at a constant temperature gradient of 10.0 K/mm. The microstructural observations of unidirectionally solidified samples show that the lamellar eutectic growth was observed in the sample solidified at a constant velocity of 1 μm/s and the rod eutectic growth at velocities higher than 10 μm/s. A microstructural transition from lamellar to rod eutectics was achieved at the intermediate velocity. The lamellar to rod eutectic transition was shown to result from the compositional change due to the presence of strong convection in the melt. The undercooling-spacing curves showed that the average eutectic spacings for the lamellar and the rod structures were 1.6 times larger than that in the minimum undercooling for a given velocity.
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    Microstructure evolution and thermal durability with coating thickness in APS thermal barrier coatings
    (2014) Lu, Z; Myoung, S W; Kim, E H; Lee, J H; Jung, Y G
    The effects of the coating thickness on the delamination or fracture behavior of thermal barrier coatings (TBCs) were investigated through the cyclic furnace thermal fatigue (CFTF) and thermal shock (TS) tests. The TBCs were prepared using a NiCrAlY bond coat and an yttria-stabilized zirconia top coat, which were formed using the air plasma spray (APS) process. The thicknesses of the top coat were 200 and 400 μm, and those of the bond coat were 100 and 200 μm. TBC samples with a thickness ratio of 2:1 in the top and bond coats were employed in the CFTF and TS tests. After CFTF for 1429 cycles, the interface microstructure of the relatively thick TBC was in a sound condition without any cracking or delamination; however, the relatively thin TBC was delaminated near the interface between the top and bond coats after 721 cycles. In the TS, the TBCs were fully delaminated (> 50%) after 140 and 194 cycles for thicknesses of 200 and 400 μm in the top coat, respectively. These observations allow us to control the thickness of TBC prepared using the APS process, and the thicker TBC is more efficient in improving thermal durability in the cyclic thermal exposure and thermal shock environments.